Scaleup of a Single-Mode Microwave Reactor
Title | Scaleup of a Single-Mode Microwave Reactor |
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Publication Type | Journal Article |
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Abstract |
Widespread use of microwave technology requires quantitative scale-up models. Currently, microwave models are typical qualitative in nature. This work focuses on rendering models quantitative and elucidating the scale-up behavior of microwave heating using numerical simulations. A commonly used bench-scale microwave reactor from the CEM Corp. (CEM Discover SP) is used for benchmarking. To enable quantitative modeling, microwave heating experiments are conducted and compared to COMSOL calculations to develop a calibration curve for the set point vs the actually delivered microwave power. Using the validated computational model, microwave-heating of various liquids in a wide range of vial sizes is investigated. The computational study shows that during the scale-up, the volumetric power absorbed passes through a maximum, whereas the energy efficiency and heating uniformity exhibit strongly nonlinear behavior. This work introduces a method for quantitative microwave models and insights into the scale-up of commercial microwave reactors.
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Year of Publication |
2020
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Journal |
Industrial and Engineering Chemistry Research
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Volume |
59
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Number of Pages |
2516-2523
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Date Published |
feb
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